Berlinite SXES spectrum, 5 keV e- beam, CSIRO 2016

Measurement details

Description SXES spectrum of Berlinite
Reference CSIRO SXES database by C. M. MacRae, N. C. Wilson, and A. Torpy, CSIRO Mineral Resources
https://spectroscopy.csiro.au/sxes
Date measured 2016-09-27
Material Berlinite [ AlPO4 ]
Specimen AlPO4 Hyper1-4 [CSIRO - Microbeam Lab standard blocks]
Related specimen P-0016 AlPO4 [CSIRO - Microbeam Lab P-mounts]. Seems to be clean. Our probe analysis is good
Technique Soft x-ray emission spectroscopy (SXES)
Instrument JEOL 8530F
Probe 5 keV electron beam
Beam current 60.1 nA
Grating 50XL
Acquisition time 720 s
Channel count 2048
Energy range 46.8109 … 170.472 eV
Intensity range 89.2461 … 2584.88 counts
Integral 501840 counts

Composition

Nominal composition of Berlinite [ AlPO4 ].
Element Atoms At% Wt%
Al 1 16.7 22.1
P 1 16.7 25.4
O 4 66.7 52.5

Measurement spectrum

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Measurement image

SXES spectrum of Berlinite