Anglesite CL/SEM spectrum, 12 keV e- beam, CSIRO 2020

Measurement details

Description CL/SEM spectrum of Anglesite
Reference Otherwise unpublished luminescence spectra measured by the CSIRO Mineral Resources Microbeam Laboratory, Clayton
https://research.csiro.au/microbeam-lab/
Date measured 2020-11-04
Material Anglesite [ PbSO4 ]
Technique Cathodoluminescence (CL), using an Electron Probe Micro-Analyser (EPMA)
Instrument JEOL 8500F
Probe 12 keV electron beam
Beam current 5 nA
Probe diameter 5 μm
Detector name OceanInsight QE Pro
Det. technology CCD, Si, Peltier cooled
Acquisition time 30 s
Channel count 1024
Energy range 1.28909 … 6.86293 eV
Intensity range 0.912613 … 99.3345 (normalised intensity)
Data filter Savitzky-Golay, 3rd order, ±20 channels
Lines Unspecified 3.182 eV (100%), 2.544 eV (48.6%)

Composition

Nominal composition of Anglesite [ PbSO4 ].
Element Atoms At% Wt%
Pb 1 16.7 68.3
O 4 66.7 21.1
S 1 16.7 10.6

Measurement spectrum

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Measurement image

CL/SEM spectrum of Anglesite