Alumina and Spinel CL/SEM measurement, 17 keV e- beam, Imashuku et al. 2017
Measurement details
| Reference | Imashuku et al. 2017 Imashuku S., Ono K., Shishido R., Suzuki S. & Wagatsuma K. (2017). Cathodoluminescence analysis for rapid identification of alumina and MgAl2O4 spinel inclusions in steels. Materials Characterization, 131, 210-216. DOI: https://doi.org/10.1016/j.matchar.2017.07.016 |
| Materials | Alumina (var. inclusion in steel) [ Al2O3 ], Spinel (var. inclusion in steel) [ MgAl2O4 ] |
| Specimen temperature | Ambient |
| Technique | Cathodoluminescence (CL), using a Scanning Electron Microscope (SEM) |
| Instrument | TECHNEX Mighty-8DXL |
| Probe | 17 keV electron beam |
| Beam current | 19 nA |
| Detector name | OceanOptics QEPRO |
| Det. technology | CCD, Si, Peltier cooled |
| Lines | Cr3+: 697 nm, Mn2+: 430 nm, 465 nm, 525 nm, 730 nm, Oxygen vacancy: 335 nm, 480 nm, Ti3+: 750 nm |