Zirconia (var. Y stabilised) SXES spectrum, 5 keV e- beam, CSIRO 2016
Measurement details
| Description | SXES spectrum of stabilised zirconia |
| Reference | CSIRO SXES database by C. M. MacRae, N. C. Wilson, and A. Torpy, CSIRO Mineral Resources https://research.csiro.au/microbeam-lab/ |
| Date measured | 2016-09-27 |
| Material | Zirconia (var. Y stabilised) [ ZrO2:Y ] |
| Specimen | ZrO2(Y) HyperI-41 [CSIRO - Microbeam Laboratory Standards] |
| Related specimen | P-0293 Zirconia [CSIRO - Microbeam Laboratory Standards]. Stabilised cubic zirconia. ex L. Cranswick CSIRO. Note: check for MgO and or Y2O3 (also Th and U) |
| Technique | Soft x-ray emission spectroscopy (SXES) |
| Instrument | JEOL 8530F |
| Probe | 5 keV electron beam |
| Beam current | 60.1 nA |
| Grating | 50XL |
| Acquisition time | 720 s |
| Channel count | 2048 |
| Energy range | 46.8109 … 170.472 eV |
| Intensity range | 100.954 … 10886.4 counts |
| Integral | 1.1068×106 counts |
Composition
| Element | Atoms | At% | Wt% |
|---|---|---|---|
| Y | 13.1 | 13.1 | 16.1 |
| Hf | 0.8 | 0.8 | 1.97 |
| Zr | 60.7 | 60.7 | 76.4 |
| O | 25.4 | 25.4 | 5.6 |
Measurement spectrum
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Measurement image
SXES spectrum of stabilised zirconia