Thulium ultraphosphate SXES spectrum, 5 keV e- beam, CSIRO 2016

Measurement details

Description SXES spectrum of Thulium ultraphosphate
Reference CSIRO SXES database by C. M. MacRae, N. C. Wilson, and A. Torpy, CSIRO Mineral Resources
https://spectroscopy.csiro.au/sxes
Date measured 2016-09-27
Material Thulium ultraphosphate [ TmP5O14 ]
Specimen TmP5O14 REEP-13 [CSIRO - Microbeam Lab standard blocks]
Related specimen REEP25-15 block [CSIRO - Microbeam Lab standard blocks]. Astimex rare earth ultraphosphate standard block (REEP25-15, Serial TU)
Technique Soft x-ray emission spectroscopy (SXES)
Instrument JEOL 8530F
Probe 5 keV electron beam
Beam current 59.8 nA
Grating 50XL
Acquisition time 720 s
Channel count 2048
Energy range 46.8109 … 170.472 eV
Intensity range 48.2014 … 2006.34 counts
Integral 565400 counts

Composition

Composition of Thulium ultraphosphate in specimen "TmP5O14 REEP-13" [CSIRO].
Element Atoms At% Wt%
Tm 1 5 30.8
P 5 25 28.3
O 14 70 40.9

Measurement spectrum

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