Thulium ultraphosphate SXES spectrum, 5 keV e- beam, CSIRO 2016
Measurement details
| Description | SXES spectrum of Thulium ultraphosphate |
| Reference | CSIRO SXES database by C. M. MacRae, N. C. Wilson, and A. Torpy, CSIRO Mineral Resources https://research.csiro.au/microbeam-lab/ |
| Date measured | 2016-09-27 |
| Material | Thulium ultraphosphate [ TmP5O14 ] |
| Specimen | TmP5O14 REEP-13 [CSIRO] |
| Related specimen | REEP25-15 block [CSIRO]. Astimex rare earth ultraphosphate standard block (REEP25-15, Serial TU) |
| Technique | Soft x-ray emission spectroscopy (SXES) |
| Instrument | JEOL 8530F |
| Probe | 5 keV electron beam |
| Beam current | 59.8 nA |
| Grating | 50XL |
| Acquisition time | 720 s |
| Channel count | 2048 |
| Energy range | 46.8109 … 170.472 eV |
| Intensity range | 48.2014 … 2006.34 counts |
| Integral | 565400 counts |
Composition
| Element | Atoms | At% | Wt% |
|---|---|---|---|
| Tm | 1 | 5 | 30.8 |
| P | 5 | 25 | 28.3 |
| O | 14 | 70 | 40.9 |
Measurement spectrum
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