Heazlewoodite SXES spectrum, 5 keV e- beam, CSIRO 2016

Measurement details

Description SXES spectrum of Heazelwoodite
Reference CSIRO SXES database by C. M. MacRae, N. C. Wilson, and A. Torpy, CSIRO Mineral Resources
https://spectroscopy.csiro.au/sxes
Date measured 2016-09-26
Material Heazlewoodite [ Ni3S2 ]
Specimen Ni3S2 Hyper2-4 [CSIRO - Microbeam Lab standard blocks]
Related specimen P-0194 Ni3S2 [CSIRO - Microbeam Lab P-mounts]
Technique Soft x-ray emission spectroscopy (SXES)
Instrument JEOL 8530F
Probe 5 keV electron beam
Beam current 99.9 nA
Grating 50XL
Acquisition time 640 s
Channel count 2048
Energy range 46.8109 … 170.472 eV
Intensity range 147.883 … 6737.51 counts
Integral 1.2549×106 counts

Composition

Nominal composition of Heazlewoodite [ Ni3S2 ].
Element Atoms At% Wt%
Ni 3 60 73.3
S 2 40 26.7

Measurement spectrum

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Measurement image

SXES spectrum of Heazelwoodite

© (C) 2016 CSIRO Mineral Resources