Titanite EDS spectrum, 20 keV e- beam, Torpy et al. 2020

Measurement details

Description EDS spectrum of Titanite
Reference Torpy et al. 2020
Torpy, A., Wilson, N., MacRae, C., Pownceby, M., Biswas, P., Rahman, M., & Zaman, M. (2020). Deciphering the Complex Mineralogy of River Sand Deposits through Clustering and Quantification of Hyperspectral X-Ray Maps. Microscopy and Microanalysis, 26(4), 768-792
https://doi.org/10.1017/S143192762000135X
Date measured 2018-05-01
Material Titanite [ CaTiSiO5 ]
Specimen Tista 2020 D4 Shaker [CSIRO], Teesta River, Bangladesh
Technique Energy dispersive x-ray spectrometry (EDS)
Instrument JEOL 8500F
Probe 20 keV electron beam
Beam current 69.64 nA
Probe diameter 2 μm
Detector name 2× Bruker XFLASH
Det. technology Silicon drift detector (SDD)
Real time 522.9 s
Live time 326.77 s
Dead time 37.5081 %
Channel count 4096
Energy range -477.548 … 19984.5 eV
Gain 4.99684 eV/channel
Intensity range 1.2675×106 counts
Integral 1.0934×108 counts
Related measurement Titanite CL spectrum, 20 keV e- beam, Torpy et al. 2020 (co-measured)

Composition

Composition from this measurement.
Element Atoms At% Wt%
Ca 1.04 12.3 20.2
Ti 1 11.8 23.2
Fe 0.0177 0.21 0.48
Si 1.08 12.8 14.7
O 5.33 62.9 41.3

Measurement spectrum

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