Apatite EDS spectrum, 20 keV e- beam, Torpy et al. 2020
Measurement spectrum
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Measurement details
| Description | EDS spectrum of Apatite, from the Tista River, Bangladesh |
| Reference | Torpy et al. 2020 Torpy, A., Wilson, N., MacRae, C., Pownceby, M., Biswas, P., Rahman, M., & Zaman, M. (2020). Deciphering the Complex Mineralogy of River Sand Deposits through Clustering and Quantification of Hyperspectral X-Ray Maps. Microscopy and Microanalysis, 26(4), 768-792 https://doi.org/10.1017/S143192762000135X |
| Date measured | 2018-05-07 |
| Material | Apatite [ Ca5(PO4)3(OH, F, Cl) ] |
| Analysis technique | Energy dispersive x-ray spectrometry (EDS) |
| Instrument | JEOL 8500F |
| Probe | 20 keV electron beam |
| Beam current | 69.95 nA |
| Probe diameter | 2 μm |
| Detector name | 2× Bruker XFLASH |
| Det. technology | Silicon drift detector (SDD) |
| Takeoff angle | 40° |
| Max. throughput | 260 kcounts/s |
| Real time | 2682.66 s |
| Live time | 1623.89 s |
| Dead time | 39.4672 % |
| Channel count | 4096 |
| Energy range | -477.548 … 19994.5 eV |
| Gain | 4.99928 eV/channel |
| Intensity range | 8.879×106 counts |
| Integral | 5.9134×108 counts |
| Related measurement | Apatite CL spectrum, 20 keV e- beam, Torpy et al. 2020 (co-measured) |
Specimen details
Specimen image
Image of a specimen of Zircon from Tista River, Bangladesh
© (C) 2020 CSIRO Mineral Resources
Composition
| Element | Atoms | At% | Wt% |
|---|---|---|---|
| H | 0.118 | 1.66 | 0.07 |
| Ca | 1.667 | 23.42 | 39.36 |
| P | 1 | 14.05 | 18.25 |
| O | 4.112 | 57.76 | 38.76 |
| F | 0.111 | 1.56 | 1.24 |
| Cl | 0.111 | 1.56 | 2.32 |