Biotite EDS spectrum, 15 keV e- beam, CSIRO 2015

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Measurement details

Description EDS spectrum of Biotite
Reference Spectra from unpublished supplementary material for: Torpy A., Wilson N.C., MacRae C.M., Barnes S., and Verrall M. (2015), Characterising drill core mineralogy by micro-XRD mapping, AMAS XIII: the 13th Biennial Australian Microbeam Analysis Symposium: program and abstracts, Eds: Karsten Goemann, Leonid Danyushevsky and Jay Thompson, University of Tasmania, Hobart, February 2015. IBSN: 978-09580408-5-3. https://nla.gov.au/nla.obj-2477868828/view
Date measured 2015-01-30
Material Biotite [ K(Mg, Fe)3AlSi3O10(OH, F)2 ]
Analysis technique Energy dispersive x-ray spectrometry (EDS)
Instrument JEOL 8500F
Probe 15 keV electron beam
Beam current 40.12 nA
Detector name 2× Bruker XFLASH
Real time 5995.68 s
Live time 4756.75 s
Dead time 20.6637 %
Channel count 3096
Energy range -475.251 … 14984 eV
Gain 4.99491 eV/channel
Intensity range 5.866×106 counts
Integral 5.0996×108 counts
Comment EDS spectrum from unpublished supplementary material.
Measurement tags Unpublished

Specimen details

Name KH-2
Owner CSIRO
Catalog ID S-15-002
Locality Kharaelakh intrusion, Noril'sk-Talnakh region, Krasnoyarsk Krai, Siberian Federal District, Russia
Type Rock fragment
Form Thin section
Other measurements CL

EDS

Specimen image

Clustered EPMA phase map of the KH-2 specimen (owner: S. Barnes, CSIRO Mineral Resources), from the Kharelakh intrusion, Noril'sk, Russia

(C) 2015 CSIRO Process Science and Engineering. All Rights reserved.


Composition

Nominal composition of Biotite [ K(Mg,Fe)3AlSi3O10(OH,F)2 ].
Element At% Wt%
H 8.1 0.41
K 4.6 9.02
Mg 11.49 14.02
Fe 2.3 6.44
Al 4.59 6.22
Si 13.79 19.44
O 53.98 43.36
F 1.15 1.1
Total 100 100